IBR-2 Pulsed Reactor — Facilities — EPSILON/SKAT  — SKAT diffractometer

The high-resolution texture diffractometer SKAT

Summary 
The SKAT is a multi-detector diffractometer consisting of three independent detector systems. Each detector system is characterized by unique scattering geometry of the detectors. Selecting the optimum scattering angle 2θ allows adaptation of the accessible d-range and resolution Δd/d to sample requirements. If desired, the wavelength range may be expanded by an additional beam chopper, which covers every second neutron pulse. 
Instrument description 
The SKAT diffractometer comprises three ring-shaped carriers, each bearing up to 19 detector-collimator units located at 2θ = 65° / 90° and 135°, respectively. The three detector systems are developed for an alternative use, detector-collimator units are exchangeable between systems. Selection of a unique scattering angle for the detectors results in identical positions of the diffraction peaks, hence, all λ- and θ- dependent corrections can be avoided.
The 2θ = 65° detector system allows texture experiments with good resolution up to a maximum lattice spacing of dmax = 6.5 Å. A single sample resolution around an axis Z at an angle of 57.5° with respect to the incident neutron beam is sufficient to cover the whole pole figure. 
The 2θ = 90° detector system allows high resolution texture experiments up to a maximum lattice spacing of dmax = 5.0 Å. A single sample resolution around an axis Z at an angle of 45.0° with respect to the incident neutron beam is sufficient to cover the whole pole figure. The goniometer angle of 45° offers the optimum conditions for the installation of uniaxial sample environments for in situ experiments. 
The 2θ = 135° detector system allows very high resolution texture experiments up to a maximum lattice spacing of dmax = 3.9 Å. Two goniometer positions (Z at 22.5° and 67.5°) are required to cover the whole pole figure. 

 

Layout of the SKAT detector systems for alternative use. 
The sample is rotated around the axis Z, for the detector system 2θ = 135° two sample positions P1 and P2 
are required. Sample movements around the X and Y axes are also possible.

 

Photograph of the SKAT with the detector system at 2θ = 90° and the goniometer for sample rotation (status December 2006)

 

Predicted resolution of the SKAT detector systems, derived from experimental data of the former neutron guide for sample rotation (status December 2006)

Instrument characteristics

Primary beam path ~ 102 m
Optional scattering angles 2θ 65° / 90° / 135°
λmax 7.0 Å / 14.6 Å*

2θ-related parameters

2θ = 65°

2θ = 90°

2θ  = 135°

dmax

6.5 Å / 13.6 Å*

5.0 Å / 10.3 Å*

3.8 Å / 7.9 Å*

Best resolution Δd/d

6.2·10-3

5.0·10-3

3.1·10-3

Secondary beam path

1.10 m

1.00 m

0.95 m


Neutron guide


Cross section: 50 mm (w) × 90 mm (h)
Radius: 13400 m
Coating: natural Ni (m = 1)
Option: chopper covering every 2nd neutron pulse


Detectors


Set of 19 3He single tube detectors
P = 4.5 bar
Ø = 60 mm


Secondary collimation


Two sets of Gd-coated soller collimators
Angular dispersion: 18' / 45'
Cross section: 55 × 55 mm2


Sample positioning

3 axes goniometer
Data acquisition system

SONIX software PC running MS Windows

* applying the primary beam chopper